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العنوان
Synthesis and reactions of some new s- triazole derivatives /
المؤلف
Hussein, Bahgat Ramadan Mahmoud.
هيئة الاعداد
باحث / بهجت رمضان محمود حسن
bahgat_mahmoud@science.sohag.edu.eg
مشرف / عبد البديع احمد جودة غطاس
abdelbadei_ghatas@science.sohag.edu.eg
مشرف / حسن محمود مصطفى
hasan.abdelmoula@science.sohag.edu.eg
مشرف / السيد عبد اللاه عبد العال
alsayed33@science.sohag.edu.eg
مشرف / السيد عبد اللاه عبد العال
alsayed33@science.sohag.edu.eg
الموضوع
triazole reactions.
تاريخ النشر
2012.
عدد الصفحات
181 p. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
Organic Chemistry
تاريخ الإجازة
31/7/2012
مكان الإجازة
جامعة سوهاج - كلية العلوم - كيمياء خاصة
الفهرس
Only 14 pages are availabe for public view

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Abstract

Alkylation of 4-anilino-5-pheny1-4h-1,2,4-triazole-3-thiol (1) with halo compounds namely: chloroacetamide , bromomalononitrile and ethy1 chloroacetate gave the corresponding sulfides 2- 7 ,respectively. compounds 6and7 underwent cyclization to afford triazolo(3,4-b) thiadiazines 8 and9 , respectively . reaction of compound 1 with hydrazine hydrate, carbondisulfide, ethy1 orthoformate, lawessons reagent (lr), ethy1 chloroformate and pheny1 isothiocynate afforded compounds 10-15, respectively. compounds 14 and 15 were cyclized to give compounds 16 and 17,respectively. thiation of compound 16 by usinglawessons reagent (lr)in xylene afforded the corresponding triazolo(3,4-b) thiadiazole - 6-thione 11.