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Abstract In this work we have prepared seven samples of COI00-~x (9.4 < x < 24.5) by using the electro-plating technique. It has been found that the surface homogeneity of the prepared materials is very sensitive to the parameters controlling the experiment. Atomic absorption spectrophotometer have been used to determinate the atomic percentage of phosphorus (at.% of P), X-ray diffraction has been used to characterize the amorphous state of the samples. It was found that the samples of x < 11 % can not be prepared in amorphous form. The dc electrical resistivity has been measured. |