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العنوان
Synthesis and characterization of Polymeric Nanocomposite Films for Nuclear Radiation Shielding \
المؤلف
Ibrahim, Marwa Freag Mahmoud.
هيئة الاعداد
باحث / مروه فريج محمود إبراهيم
مشرف / هناء حسن أبو جبل
hanaaag@hotmail.com
مشرف / محمد حسن محمد حسن
مشرف / إبراهيم محمد الشربينى عبد الحليم
مناقش / سعيد عبد المجيد عجمي
sagamy@link.net
مناقش / عمرو سعد جلال
الموضوع
Nuclear Engineering.
تاريخ النشر
2018.
عدد الصفحات
78 p. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
الهندسة (متفرقات)
تاريخ الإجازة
1/2/2018
مكان الإجازة
جامعة الاسكندريه - كلية الهندسة - الهندسة النووية والاشعاعية
الفهرس
Only 14 pages are availabe for public view

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Abstract

In this research, Lead-free polymer composites have been designed to be used as a Gamma radiation shielding and protection agent, reinforced with different concentrations of nanomaterials (10-30-50) %wt. by using Polyvinyl alcohol (PVA) as a matrix material with various metal oxides as reinforcing agents, such as Iron (III) oxide, Graphene oxide, Zinc oxide. The morphology of the samples was investigated using X-ray Diffraction (XRD), Scanning Electron Microscope (SEM) and Transmission Electron Microscopy (TEM), Fourier transform infrared spectroscopy (FTIR) has been used to examine the presence of hydrogen bonding and its effect on crystallinity. The thermal properties were examined by (TGA-DSC), and the size of nanoparticles has been determined using Zeta sizer. Raman Spectroscopy characterized the Go nanocomposite film. Following to the above steps, the linear attenuation coefficient of different polymeric nanomaterial has been experimentally calculated using the photons of gamma rays emitted from radioactive sources (Cs137) at energy (662) KeV by using gamma spectrometer which is connected with sodium iodide activated with thallium detector, as a function of the absorber thickness and energy. Comparing the linear attenuation parameters has shown that the nanocomposite of magnetite nanoparticles and PVA film is a promising radiation material, in reasonable thickness and weight, with various industrial applications.